trendsetter37
The Living Force
hlat said:Laura said:hlat said:FYI people in the US cannot buy at retail Lugol's over 5% and over 1 ounce due to DEA recordkeeping regulations.
_http://www.jcrows.com/iodinealert.html
Lugol's Solution is a 5 percent aqueous solution of iodine in combination with 10 percent potassium iodide.
...
Because of the numerous legitimate uses and small quantities involved, DEA is adding a provision to this final rule that will exempt Lugol's Solution when packaged in bottles/containers of one-fluid-ounce (30 ml) or smaller, and involve distribution of only a single package per transaction.
I am getting discouraged in making my own Lugol's because I am not finding a supplier with a certificate of analysis for USP grade iodine and potassium iodide. Does anyone have any ideas or suggestions in finding such a supplier?
As an alternative, I am considering buying a 5 gallon container of 2% Lugol's. That's $689.95 for 640 ounces, or $1.08 per ounce.
_http://www.jcrowsmarketplace.com/5gallonbulkdrumwithspigotlugolssolution2includesshipping.aspx
http://www.amazon.com/gp/product/B013Q1Y514
http://www.amazon.com/gp/product/B00NAD3N3K
That seller of iodine does not have a certificate of analysis, and is not able to substantiate its claim of purity.
That seller is also evading DEA regulations for the exemption level of 5% by selling a 7% bottle on ebay.
_http://www.ebay.com/itm/Lugols-iodine-solution-1-fluid-ounce-30ml-7-iodine-/320675830716
The general DEA limit is 2.2%, with an exemption for 5% 1 ounce bottle.
_http://www.jcrows.com/iodinealert.html
This rulemaking establishes regulatory controls that will apply to iodine crystals and iodine chemical mixtures that contain greater than 2.2 percent iodine.
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This final rulemaking includes a waiver of the registration requirement under 21 CFR 1309.24 for "Lugol's Solution (consisting of 5 percent iodine and 10 percent potassium iodide in an aqueous solution) in original manufacturer's packaging of one-fluid-ounce (30 ml) or less per package." Additionally, this rulemaking includes an exclusion from the definition of regulated transaction under 21 CFR 1310.08 for "Domestic and international transactions of Lugol's Solution (consisting of 5 percent iodine and 10 percent potassium iodide in an aqueous solution) in original manufacturer's packaging of one-fluid-ounce (30 ml) or less, and no greater than one package/bottle per transaction."
Those two red flags are enough for me to avoid any products by this seller unless it addresses my concerns.
Also just to add that second link from amazon for the 1lb of potassium iodide has the incorrect percentage of potassium and iodide. It states that there is 31% K and 69% iodide when in actuality potassium iodide should be 24% potassium and 76% iodide. That is a pretty big discrepancy for it to be posted front and center on the label like that.
KI mwt. = 166.06
K = 39.0983 => 39.0983 / 166.06 = 0.2355 * 100 ~ 24%
I = 126.9 => 126.9 / 166.06 = 0.7644 * 100 ~ 76%
But maybe that is just a clerical oversight? And since you all haven't had any issues with it then maybe it's ok? I haven't found any other sources better than those two if one is going to make their own solution. In any case I should be able to finish the book tonight, I'm kind of excited